Advanced Techniques of Analysis and Characterization

上海交通大学硕士研究生课程教学大纲

 

课程基本信息(Course Information

课程代码

Course Code

 

*学时

Credit Hours

32

*学分

Credits

2

*课程名称

Course Name

(中文)先进分析与表征技术

(英文)Advanced Techniques of Analysis and Characterization

课程性质

(Course Type)

专业选修课 Elective Courses

授课语言

(Language of Instruction)

英文/English

*开课院系

School

中英国际低碳学院China-UK Low Carbon College

先修课程

Prerequisite

/None

授课教师

Teacher

纪亚 / Ji Ya

课程网址

(Course Webpage)

 

 

*课程简介(Description

《先进分析与表征技术》(英文课程)将介绍在绿色低碳可持续发展时代背景下环境和能源领域分析与表征技术的重要性、各种先进技术的基本原理和应用、未来发展趋势等。该课程将涵盖光谱技术、色谱技术、电化学分析、表面分析技术等。本课程还将介绍各类分析与表征技术对环境污染物、能源材料等研究对象的适用性和分析过程,同时介绍分析与表征技术中的绿色样品处理技术和绿色分析表征技术。该课程的教学将帮助学生理解和认识绿色低碳框架下分析与表征技术的重要性和基本理论、分析表征仪器的原理和构造、定性定量分析方法及应用,培养学生应用先进分析与表征技术分析评估环境污染物和能量材料的能力,使学生了解并掌握先进分析与表征技术与绿色环境、低碳能源的关系。

*课程简介(Description

The course of Advanced Techniques of Analysis and Characterization will address the significance of analysis and characterization in fields of environment and energy under low carbon era, fundamental theories and applications of various advanced techniques, and potential future trends for analysis and characterization techniques. The main contents of this course include spectroscopic techniques, chromatographic techniques, electrochemical techniques and surface analysis techniques. This course will also introduce applicability and process of analysis and characterization for environmental pollutants and energy materials by various techniques, green sample preparation techniques and green analysis techniques. This course will help the students to understand the significance of analysis and characterization techniques in global low carbon transition, principles and instruments of advanced techniques for analysis and characterization. Qualitative and quantitative analysis methods as well as applications will be also covered. Through this course, the students will have the ability to analyze environmental pollutants and energy materials by different advanced techniques and understand the relations between advanced techniques and green environment and low carbon energy.

课程教学大纲(course syllabus

*学习目标

  • 理解绿色低碳框架下分析与表征技术的重要性和基本理论;
  • 掌握应用先进分析与表征技术分析评估环境污染物和能量材料的能力;
  • 了解并掌握先进分析与表征技术与绿色环境、低碳能源的关系;

*Learning Outcomes

  • Understand the importance and basic theories of analysis and characterization technologies within the green and low-carbon framework;
  • Master the ability to analyze and evaluate environmental pollutants and energy materials using advanced analysis and characterization technologies;
  • Understand and grasp the relationship between advanced analysis and characterization technologies and the green environment as well as low-carbon energy.

*教学内容、进度安排及要求

(Class Schedule

& Requirements)

教学内容

学时

教学方式

作业及要求

基本要求

考查方式

先进分析与表征技术绪论

2

多媒体授课

课后归纳总结

了解在绿色低碳可持续发展的时代背景下分析与表征的重要性和课程框架

课堂提问与讨论

原子光谱技术

3

多媒体授课

随堂测验

了解原子吸收光谱、原子发射光谱、质谱等技术的基本理论、仪器、定性定量方法和应用

课堂提问与讨论

分子光谱技术

3

多媒体授课/实验室教学

课后作业

了解红外吸收光谱、紫外-可见吸收光谱、拉曼光谱、荧光光谱、核磁共振波谱等技术的基本理论、仪器、定性定量方法和应用

课堂提问与讨论

气相色谱技术

3

多媒体授课

课后归纳总

结本章内容

了解色谱技术分类、基本理论、仪器、定性定量方法和应用、气相色谱工作原理

课堂提问与讨论

高效液相色谱技术

3

多媒体授课

随堂测验

了解正相和反相液相色谱的基本理论、仪器、定性定量方法和应用

课堂提问与讨论

超临界流体色谱和毛细管电泳技术

3

多媒体授课

课后归纳总

结本章内容

了解超临界流体色谱和毛细管电泳技术的基本理论、仪器、定性定量方法和应用

课堂提问与讨论

电化学分析技术

2

多媒体授课

课后作业

了解各类电化学分析技术包括电流传感器、伏安传感器和电导传感器等的基本理论、仪器、定性定量方法和应用

课堂提问与讨论

热分析技术

2

多媒体授课/实验室教学

随堂测验

了解热重分析、差热分析、差示扫描量热法技术的基本理论、仪器、定性定量方法和应用

课堂提问与讨论

电子显微镜技术

2

多媒体授课

课后归纳总

结本章内容

了解各类电子显微镜技术的基本理论、仪器、定性定量方法和应用

课堂提问与讨论

环境污染物的分析

2

多媒体授课

课后作业

了解环境污染物的特点、分类及其分析方法

课堂提问与讨论

能源材料的表征

2

多媒体授课

随堂测验

了解能源材料的特点、分类及其表征方法

课堂提问与讨论

绿色样品处理和分析表征技术

2

多媒体授课

随堂测验

了解分析表征过程中的绿色样品处理技术和分析表征技术

课堂提问与讨论

学生选题

3

课堂交流讨论

总结归纳

学生展示先进分析表征技术的最近研究进展和应用案例

课堂展示

 

Content

Teaching Hours

Teaching Methods

Assignment

Requirements

Assessment

Introduction to advanced techniques of analysis and characterization

2

Lecture/PPT

Summary

Understand the significance of techniques of analysis and characterization in global low carbon transition and whole course frameworks

Questions and Discussions

Atomic Spectroscopy

3

Lecture/PPT

Quiz

Understand atomic spectroscopy techniques including atomic absorption spectroscopy, atomic emission spectroscopy and mass spectrometry in terms of fundamental theories, instruments, analysis methods and applications

Questions and Discussions

Molecular Spectroscopy

3

Lecture/PPT/Lab

Homework

Understand molecular spectroscopy techniques including  ultraviolet-visible spectroscopy, fluorescence spectroscopy, infrared spectroscopy, raman spectroscopy and nuclear magnetic resonance in terms of fundamental theories, instruments, analysis methods and applications

Questions and Discussions

Gas Chromatography

3

Lecture/PPT

Summary

Understand classifications, fundamental theories, instruments, analysis methods and applications of chromatography as well as working principle of gas chromatography

Questions and Discussions

High-Performance Liquid Chromatography

3

Lecture/PPT

Quiz

Understand high-performance liquid chromatography including normal phase and reverse phase in terms of fundamental theories, instruments, analysis methods and applications

Questions and Discussions

Supercritical Fluid Chromatography And Capillary Electrophoresis

3

Lecture/PPT

Summary

Understand supercritical fluid chromatography and capillary electrophoresis in terms of fundamental theories, instruments, analysis methods and applications

Questions and Discussions

Electrochemical Analysis Techniques

2

Lecture/PPT

Homework

Understand electrochemical techniques including amperometric sensors, voltammetric sensors and conductometric sensors in terms of fundamental theories, instruments, analysis methods and applications

Questions and Discussions

Thermal Analysis Techniques

2

Lecture/PPT/Lab

Quiz

Understand thermal analysis techniques including a thermogravimetry analysis, differential thermal analysis and differential scanning calorimetry in terms of fundamental theories, instruments, analysis methods and applications

Questions and Discussions

Electron Microscopy Techniques

2

Lecture/PPT

Summary

Understand various electron microscopy techniques in terms of fundamental theories, instruments, analysis methods and applications

Questions and Discussions

Analysis of Environmental Pollutants

2

Lecture/PPT

Homework

Understand classification, characteristics and analysis methods of environmental pollutants

Questions and Discussions

Characterization of Energy Materials

2

Lecture/PPT

Quiz

Understand classification, characteristics and characterization methods of energy materials

Questions and Discussions

Green Sample Preparation and Analytical Techniques

2

Lecture/PPT

Quiz

Understand green chemistry and green analytical chemistry such as green sample preparation and analytical techniques

Questions and Discussions

 

 

 

 

Student Presentation

3

PPT presentation

Summary

Understand the latest progress of various techniques in research areas and practical cases

Presentation

 

*考核方式

(Grading)

出勤:20%, 随堂测验和课后作业:20%, 选题课堂展示:20%, 期末考试:40%

Attendance (20%), Quiz and homework (20%), Presentation (20%), Final exam (40%)

*教材或参考资料

(Textbooks & Other Materials)

1)    Principles of instrumental analysis7th edition, Douglas A. Skoog, F. James Holler, Stanley R. Crouch, Cengage Learning, 2017, ISBN: ‎ 9781305577213.

2)    Modern Environmental Analysis Techniques for Pollutants, Mustansar Hussain, Chaudhery,  San Diego: Elsevier, 2019, ISBN: 9780128169346

3)    Characterization of materials, Elton N Kaufmann, Hoboken, NJ: John Wiley and Sons 2003, ISBN: 9780471266969.

4)    《新材料表征技术》,张霞主编,华东理工大学出版社,2012ISBN: 9787562833413.

5)    《仪器分析》,方惠群、于俊生、史坚主编,科学出版社,2002ISBN: 9787030099020

6)    《现代环境分析技术》(第二版),陈玲、郜洪文主编,科学出版社,2013ISBN9787030379610.

其它

More

 

备注

Notes

 

               

 

备注说明:

1.课程大纲一般为教师网上填写,填写要求会自动提示;对于新开课程,需要填着纸质大纲,并经院系教学委员会或专业委员会通过。

2.带*内容为必填项。

3.课程简介字数为300-500字;课程大纲以表述清楚教学安排为宜,字数不限。